Method for producing malononitrile

A process for preparing propanedinitrile includes feeding, 1,1,2-trichloroethane, anhydrous AlCl3, biethylamine hydrochloride, pyridine and phosphorus into oxychloride reactor, adding cyanoacetylamine, and reflux reaction. Its advantage is high yield (93-98%).

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Bibliographische Detailangaben
Hauptverfasser: XINGGEN WANG, ZONGTAO WU, JIAN ZHOU
Format: Patent
Sprache:eng
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Zusammenfassung:A process for preparing propanedinitrile includes feeding, 1,1,2-trichloroethane, anhydrous AlCl3, biethylamine hydrochloride, pyridine and phosphorus into oxychloride reactor, adding cyanoacetylamine, and reflux reaction. Its advantage is high yield (93-98%).