Method for preparing 1, 3-propylene glycol from 3-chloropropene

The invention relates to a method for preparing 1, 3-propylene glycol from 3-chloropropene, which comprises the steps of hydrolysis, concentration, oxidation, hydrogenation and the like. The preparation process is simple to operate, the reaction condition is mild, the yield reaches 90% or above, and...

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Bibliographische Detailangaben
Hauptverfasser: FANG XIN, LAI WANYI, YANG HENGZE, FU BING, LI WENHUI, YAN XIANG, TONG LIYAN, XIA SHA
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention relates to a method for preparing 1, 3-propylene glycol from 3-chloropropene, which comprises the steps of hydrolysis, concentration, oxidation, hydrogenation and the like. The preparation process is simple to operate, the reaction condition is mild, the yield reaches 90% or above, and the 1, 3-propylene glycol content of the 1, 3-propylene glycol crude product reaches 30% or above. 本发明涉及一种由3-氯丙烯制备1,3-丙二醇的方法,该制备方法包括水解、浓缩、氧化与氢化等步骤。本发明制备工艺操作简单,反应条件温和,收率达到90%以上,1,3-丙二醇粗品的1,3-丙二醇含量达到30%以上。