Method for determining 46 antibiotics in water based on solid phase extraction-ultra-high performance liquid chromatography-electrostatic field orbitrap mass spectrometry
The invention belongs to the field of water quality detection, and particularly relates to a method for determining 46 antibiotics in water based on solid phase extraction (SPE)-ultra-high performance liquid chromatography (UPLC)-electrostatic field orbitrap mass spectrometry (Q-orbitrap). The metho...
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creator | XIONG DAWEI HE XIANGKE GAO CUILING WANG YUE WANG TIAN LI GUIXIAO |
description | The invention belongs to the field of water quality detection, and particularly relates to a method for determining 46 antibiotics in water based on solid phase extraction (SPE)-ultra-high performance liquid chromatography (UPLC)-electrostatic field orbitrap mass spectrometry (Q-orbitrap). The method comprises the following steps: firstly, preparing a standard solution; then carrying out sample treatment; and finally, detecting by adopting ultra-high performance liquid chromatography-electrostatic field orbitrap mass spectrometry. Compared with the prior art, the method for detecting the 46 antibiotics in the environmental water by using the ultra-high performance liquid chromatography (UPLC)-electrostatic field orbitrap mass spectrometry (Q-orbitrap) is established, compared with the prior art, the method can cover more types and numbers of target objects, and the pretreatment method provided by the invention can effectively improve the extraction efficiency of the target objects, so that the method can be u |
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subjects | INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES MEASURING PHYSICS TESTING |
title | Method for determining 46 antibiotics in water based on solid phase extraction-ultra-high performance liquid chromatography-electrostatic field orbitrap mass spectrometry |
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