Carbon-doped composite metal oxide oxygen evolution anode for electrolyzing carbon dioxide and preparation method of carbon-doped composite metal oxide oxygen evolution anode

The invention belongs to the technical field of carbon dioxide electrolysis oxygen evolution anode preparation, and particularly relates to a porous-structure carbon-doped composite metal oxide oxygen evolution anode for carbon dioxide electrolysis and a preparation method thereof.The preparation me...

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Hauptverfasser: YIN YANGFAN, WANG XIUPING, GAO LIXIAO, GAO CHUNYUN, LIU JIAN, ZHANG ZAILEI, REN LEI, HE JIANSHE, AI LEI, SUN LEI, ZHANG PENG, WEN YAOSHUN, ZHANG YAN, MENG XUNBIAO, JI YUANYUAN, KANG PENG, LUAN JIALIN
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention belongs to the technical field of carbon dioxide electrolysis oxygen evolution anode preparation, and particularly relates to a porous-structure carbon-doped composite metal oxide oxygen evolution anode for carbon dioxide electrolysis and a preparation method thereof.The preparation method comprises the following steps that S1, a titanium substrate is pretreated, specifically, the titanium substrate is taken and subjected to alkali washing, sand blasting, acid pickling, water washing and drying in sequence for use; s2, preparation of a precursor solution: dissolving an iridium platinum ruthenium source, a transition metal source and a carbon source in a solvent to obtain the precursor solution; s3, coating and heat treatment of a precursor solution: i) taking a part of the precursor solution, uniformly coating the surface of the pretreated titanium substrate with the precursor solution, and then sequentially performing drying, aerobic low-temperature sintering and cooling; ii) repeating the step