Preparation method of propenyloxy product

The invention discloses a preparation method of a propenyloxy product, which comprises the following steps: mixing allyloxy trimethylsilane with tetrabutylammonium fluoride, and then adding into substrate molecules for substitution reaction to generate the propenyloxy product. The raw material allyl...

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Hauptverfasser: WANG SIMING, YANG XIAOLU, WU JUNJIE, HUANG DEXIAN, HUANG YANDUAN
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention discloses a preparation method of a propenyloxy product, which comprises the following steps: mixing allyloxy trimethylsilane with tetrabutylammonium fluoride, and then adding into substrate molecules for substitution reaction to generate the propenyloxy product. The raw material allyloxytrimethylsilane used in the invention is not a highly toxic control product, and compared with controlled allyl alcohol, the raw material allyloxytrimethylsilane is easy to obtain and has environmental protection value; in the preparation method, allyloxytrimethylsilane is unprotected by tetrabutylammonium fluoride, allyl alcohol is generated in situ and directly participates in a substitution reaction, the generated allyl alcohol has no opportunity to form high-toxicity and unstable acrolein, and the preparation process is safe and environment-friendly. And the preparation method is simple, mild in reaction and easy for industrial production. 本发明公开了一种丙烯氧基产物的制备方法,包括将烯丙氧基三甲硅烷与四丁基氟化铵混合后,再加入到底物分子中进行取代反应生成丙烯氧基产物。本发明