Quality determination method for volatile medicine of tracheitis rubber paste and application of quality determination method

The invention relates to a tracheitis rubber paste volatile drug quality determination method and application thereof, and effectively solves the problems of determination of volatile drug content in tracheitis rubber paste and guarantee of product quality and curative effect, chromatographic condit...

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Bibliographische Detailangaben
Hauptverfasser: LI ZONGRUI, CHENG BAODONG, GE YONGMING, XIONG WEI, ZHANG CHUNXIA, LI TIANTIAN, HUANG YIFAN
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention relates to a tracheitis rubber paste volatile drug quality determination method and application thereof, and effectively solves the problems of determination of volatile drug content in tracheitis rubber paste and guarantee of product quality and curative effect, chromatographic condition and system applicability test: a capillary column with a polyethylene glycol 20000 stationary phase is adopted, temperature programming, split sample introduction and FID detection are adopted, and the content of volatile drugs in tracheitis rubber paste is determined. The carrier gas is nitrogen; taking naphthalene to prepare an internal standard solution; respectively preparing camphor, menthol, borneol, isoborneol, methyl salicylate and alpha-pinene solutions, placing the solutions in the same measuring flask, adding the internal standard solution, and diluting with ethyl acetate to obtain a reference substance solution; adding water into the tracheitis rubber paste, heating, refluxing and extracting, adding