Novel method for efficiently synthesizing phenylalkyl ether
The invention belongs to the technical field of organic synthesis, and particularly relates to a novel method for efficiently synthesizing phenylalkyl ether, which comprises the following steps: (1) adding phenol and alkyl carbonate into a reaction tank, and stirring to uniformly mix; and (2) convey...
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Format: | Patent |
Sprache: | chi ; eng |
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Zusammenfassung: | The invention belongs to the technical field of organic synthesis, and particularly relates to a novel method for efficiently synthesizing phenylalkyl ether, which comprises the following steps: (1) adding phenol and alkyl carbonate into a reaction tank, and stirring to uniformly mix; and (2) conveying the mixed raw material liquid into a fixed bed reactor filled with a catalyst through a constant-flux pump for reaction, introducing nitrogen in the whole reaction process, and carrying out condensation and gas-liquid separation on the reaction product, and sampling for analysis. The continuous flow fixed bed reactor is adopted, on the basis of a certain amount of catalyst, complete conversion of phenol can be achieved, alkyl carbonate can be recycled, the production cost is greatly reduced, high-purity phenylalkyl ether can be obtained, and the synthesis method is efficient, low in energy consumption and wide in application prospect.
本申请属于有机合成技术领域,具体为一种高效合成苯烷基醚的新方法,制备步骤如下:(1)向反应罐中加入苯酚和碳酸烷基酯,搅拌使其混合均匀;(2)将混合原料液通 |
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