Preparation method of anisole compound
The invention belongs to the field of catalytic material preparation and organic synthesis, and discloses a preparation method of an anisole compound. According to the method, the Fe-coated Ag/TiO2 catalyst is used for performing selective hydrodeoxygenation treatment on the syringol for the first t...
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Format: | Patent |
Sprache: | chi ; eng |
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Zusammenfassung: | The invention belongs to the field of catalytic material preparation and organic synthesis, and discloses a preparation method of an anisole compound. According to the method, the Fe-coated Ag/TiO2 catalyst is used for performing selective hydrodeoxygenation treatment on the syringol for the first time, so that synthesis of the final product anisole compound is realized. The Fe (at) Ag/TiO2 catalyst is used, reduction treatment is not needed, and the selectivity of the anisole compound in the final reaction product is larger than 90%. The reaction temperature is controlled to be 473-673K, the syringol can realize hydrogenation reaction, and complete conversion can be realized as quickly as possible when the reaction temperature is 673K. The catalyst provided by the invention is simple in preparation method, free of reduction treatment, good in reaction performance and high in product selectivity.
本发明属于催化材料制备和有机合成领域,公开了一种苯甲醚化合物的制备方法。本发明首次使用Fe@Ag/TiO2催化剂对紫丁香醇进行选择加氢脱氧处理,实现最终产物苯甲醚化合物的合成。本发明使用Fe@Ag/TiO2催化剂无需与还原处理, |
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