Thin-layer identification method for pharbitis seed sample

The invention relates to a thin-layer identification method for a pharbitis seed sample. The thin-layer identification method comprises the following steps: preparing a test solution, preparing a reference medicinal material solution and a reference substance solution, and carrying out thin-layer id...

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Hauptverfasser: GU QINYING, ZHANG YUJING, ZHAI YANJUAN, GUO KEJIA, CHEN SHENGJUN, PU XIANGLAN, GU CHAO, ZHANG YUNTIAN, GUO XINGYU, XIE JIAYING, LI SONG, ZHOU HAIQIN
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention relates to a thin-layer identification method for a pharbitis seed sample. The thin-layer identification method comprises the following steps: preparing a test solution, preparing a reference medicinal material solution and a reference substance solution, and carrying out thin-layer identification. A test solution, a reference medicinal material solution and a reference substance solution are obtained by adopting a simple, convenient and rapid pretreatment method, are respectively dripped on the same thin-layer plate, and are developed by using a suitable developing solvent to obtain a multi-information morning glory seed thin-layer chromatogram. The method is simple, convenient and rapid to operate, good in chromatographic spot separation degree, low in detection cost, safe, environment-friendly and more beneficial to quality supervision of the semen pharbitidis sample. 本发明涉及一种牵牛子样品的薄层鉴别方法,包括供试品溶液制备、对照药材溶液和对照品溶液制备、薄层鉴别步骤。本发明采用简便、快捷的前处理方法得到供试品溶液、对照药材溶液与对照品溶液,分别点于同一块薄层板上,用适宜展开剂展开,得到多信息的牵牛子薄层色谱图。该