Method for purifying crude tellurium

Method for purifying crude tellurium

The invention provides a crude tellurium purification method, and belongs to the field of high-purity metal preparation. The invention provides a purification method of crude tellurium. The purification method comprises the following steps: immersing a crystallizer into tellurium melt obtained by me...

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Hauptverfasser: LUO HUAN, XIONG HENG, WANG FEI, XU BAOQIANG, ZHA GUOZHENG, JIANG WENLONG, TIAN YANG, WU JIAN, DONG CHAOWANG, LIU DACHUN, KONG LINGXIN, YANG BIN, LI YIFU, LUO QIJIN, KONG XIANGFENG
Format: Patent
Sprache:chi ; eng
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CHEMISTRY
COMPOUNDS THEREOF
INORGANIC CHEMISTRY
METALLURGY
NON-METALLIC ELEMENTS
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creator LUO HUAN
XIONG HENG
WANG FEI
XU BAOQIANG
ZHA GUOZHENG
JIANG WENLONG
TIAN YANG
WU JIAN
DONG CHAOWANG
LIU DACHUN
KONG LINGXIN
YANG BIN
LI YIFU
LUO QIJIN
KONG XIANGFENG
description The invention provides a crude tellurium purification method, and belongs to the field of high-purity metal preparation. The invention provides a purification method of crude tellurium. The purification method comprises the following steps: immersing a crystallizer into tellurium melt obtained by melting crude tellurium for rotary crystallization; the temperature of the crystallizer is lower than that of the tellurium melt during rotary crystallization. Thinning of a liquid-solid interface solute boundary layer is achieved through interface shearing force generated by tellurium melt rotation, impurities are forcibly removed from the boundary layer, and therefore high-purity tellurium is crystallized; the temperature gradient of a liquid-phase region near a liquid-solid interface is increased through rotation of the crucible, and crystallization is quicker due to increase of the temperature gradient, so that the purification efficiency is improved. The result of the embodiment shows that the purification metho
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The invention provides a purification method of crude tellurium. The purification method comprises the following steps: immersing a crystallizer into tellurium melt obtained by melting crude tellurium for rotary crystallization; the temperature of the crystallizer is lower than that of the tellurium melt during rotary crystallization. Thinning of a liquid-solid interface solute boundary layer is achieved through interface shearing force generated by tellurium melt rotation, impurities are forcibly removed from the boundary layer, and therefore high-purity tellurium is crystallized; the temperature gradient of a liquid-phase region near a liquid-solid interface is increased through rotation of the crucible, and crystallization is quicker due to increase of the temperature gradient, so that the purification efficiency is improved. 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subjects CHEMISTRY
COMPOUNDS THEREOF
INORGANIC CHEMISTRY
METALLURGY
NON-METALLIC ELEMENTS
title Method for purifying crude tellurium
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