Method for producing dibenzylamine
The invention provides a preparation method of dibenzylamine, which comprises the following steps: adding benzonitrile into a high-pressure reaction kettle, mixing with a reaction solvent, carrying out hydrogenation reaction under the action of a cerium oxide loaded ruthenium-iron bimetallic catalys...
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Format: | Patent |
Sprache: | chi ; eng |
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Zusammenfassung: | The invention provides a preparation method of dibenzylamine, which comprises the following steps: adding benzonitrile into a high-pressure reaction kettle, mixing with a reaction solvent, carrying out hydrogenation reaction under the action of a cerium oxide loaded ruthenium-iron bimetallic catalyst to prepare a reaction crude product, cooling and filtering the catalyst, and rectifying and purifying to obtain a dibenzylamine finished product. The method is mild in reaction condition and high in atom utilization rate, and meets clean and green production requirements.
本发明提供了一种二苄胺的制造方法,通过在高压反应釜中,加入苯甲腈与反应溶剂混合,在氧化铈负载的钌-铁双金属催化剂的作用下进行加氢反应,制得反应粗品,经冷却过滤催化剂后,精馏提纯得到二苄胺成品。该方法反应条件温和、原子利用率高,符合清洁、绿色生产要求。 |
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