Quickly-cured vitrimer resin and preparation method thereof

The invention provides rapidly-cured vitrimer resin and a preparation method thereof.The preparation method comprises the following steps that 10-100 parts of an acid curing agent and 100 parts of epoxy resin are mixed, the mixture is stirred to react for 20-180 minutes at the temperature of 60-100...

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Bibliographische Detailangaben
Hauptverfasser: ZHU MINJIE, WEI LONGSHA, YAN YIWU
Format: Patent
Sprache:chi ; eng
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Beschreibung
Zusammenfassung:The invention provides rapidly-cured vitrimer resin and a preparation method thereof.The preparation method comprises the following steps that 10-100 parts of an acid curing agent and 100 parts of epoxy resin are mixed, the mixture is stirred to react for 20-180 minutes at the temperature of 60-100 DEG C and cooled to the room temperature, and pre-cured resin A still having flowability is obtained; mixing 0.1-10 parts of an amine curing agent, 0.1-10 parts of an accelerant and 0.1-5 parts of a polymerization inhibitor with the resin A, and stirring at 20-60 DEG C for 10-60 minutes to obtain resin B; and pouring the resin B into a mold, and curing for 10-30 minutes under the conditions that the pressure is 1-10 MPa and the temperature is 120-160 DEG C, so as to obtain the vitrimer resin cured product. By adopting the technical scheme of the invention, rapid curing can be realized, and the cured resin has self-repairing capability under a heating condition. 本发明提供了一种快速固化的vitrimer树脂及其制备方法,该制备方法包括如下步骤:将10-100份酸类固化