Method for recycling dimethylamine hydrochloride from methyl cyclopentenolone wastewater
The invention provides a method for recycling dimethylamine hydrochloride from methyl cyclopentenolone wastewater, and belongs to the technical field of comprehensive utilization of wastewater. The method is simple in operation steps, solves the problems of excessive reaction tail gas and high cost...
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| creator | QIN JILOU CHEN HAIBING GONG XI CHENG XIAOTAO QIAN QINGHUA |
| description | The invention provides a method for recycling dimethylamine hydrochloride from methyl cyclopentenolone wastewater, and belongs to the technical field of comprehensive utilization of wastewater. The method is simple in operation steps, solves the problems of excessive reaction tail gas and high cost in the prior art, and comprises the following steps: step 1, collecting the methyl cyclopentenolone wastewater, feeding the methyl cyclopentenolone wastewater into a decoloration kettle, adding activated carbon, stirring for decoloration, and centrifuging to remove the activated carbon to obtain the decolorized methyl cyclopentenolone wastewater; and 2, transferring the decolorized methyl cyclopentenolone wastewater obtained in the step 1 into a salifying kettle, concentrating to obtain a concentrated ammonium salt solution, cooling and crystallizing to obtain dimethylamine hydrochloride crystals, adding equal amount of formaldehyde into the recovered dimethylamine hydrochloride, and pumping into an amination kettl |
| format | Patent |
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The method is simple in operation steps, solves the problems of excessive reaction tail gas and high cost in the prior art, and comprises the following steps: step 1, collecting the methyl cyclopentenolone wastewater, feeding the methyl cyclopentenolone wastewater into a decoloration kettle, adding activated carbon, stirring for decoloration, and centrifuging to remove the activated carbon to obtain the decolorized methyl cyclopentenolone wastewater; and 2, transferring the decolorized methyl cyclopentenolone wastewater obtained in the step 1 into a salifying kettle, concentrating to obtain a concentrated ammonium salt solution, cooling and crystallizing to obtain dimethylamine hydrochloride crystals, adding equal amount of formaldehyde into the recovered dimethylamine hydrochloride, and pumping into an amination kettl</description><language>chi ; eng</language><subject>ACYCLIC OR CARBOCYCLIC COMPOUNDS ; CHEMISTRY ; METALLURGY ; ORGANIC CHEMISTRY ; TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE</subject><creationdate>2024</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20240326&DB=EPODOC&CC=CN&NR=117756647A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25542,76289</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20240326&DB=EPODOC&CC=CN&NR=117756647A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>QIN JILOU</creatorcontrib><creatorcontrib>CHEN HAIBING</creatorcontrib><creatorcontrib>GONG XI</creatorcontrib><creatorcontrib>CHENG XIAOTAO</creatorcontrib><creatorcontrib>QIAN QINGHUA</creatorcontrib><title>Method for recycling dimethylamine hydrochloride from methyl cyclopentenolone wastewater</title><description>The invention provides a method for recycling dimethylamine hydrochloride from methyl cyclopentenolone wastewater, and belongs to the technical field of comprehensive utilization of wastewater. 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The method is simple in operation steps, solves the problems of excessive reaction tail gas and high cost in the prior art, and comprises the following steps: step 1, collecting the methyl cyclopentenolone wastewater, feeding the methyl cyclopentenolone wastewater into a decoloration kettle, adding activated carbon, stirring for decoloration, and centrifuging to remove the activated carbon to obtain the decolorized methyl cyclopentenolone wastewater; and 2, transferring the decolorized methyl cyclopentenolone wastewater obtained in the step 1 into a salifying kettle, concentrating to obtain a concentrated ammonium salt solution, cooling and crystallizing to obtain dimethylamine hydrochloride crystals, adding equal amount of formaldehyde into the recovered dimethylamine hydrochloride, and pumping into an amination kettl</abstract><oa>free_for_read</oa></addata></record> |
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| subjects | ACYCLIC OR CARBOCYCLIC COMPOUNDS CHEMISTRY METALLURGY ORGANIC CHEMISTRY TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE |
| title | Method for recycling dimethylamine hydrochloride from methyl cyclopentenolone wastewater |
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