Biquaternary ammonium bisulfonate degreasing agent as well as synthesis method and application thereof
The invention belongs to the technical field of sewage treatment, and particularly relates to a biquaternary ammonium bisulfonate degreasing agent as well as a synthesis method and application thereof. The synthesis method comprises the following steps: adding piperazine, sodium p-hydroxybenzenesulf...
Gespeichert in:
Hauptverfasser: | , , , , , , , , , |
---|---|
Format: | Patent |
Sprache: | chi ; eng |
Schlagworte: | |
Online-Zugang: | Volltext bestellen |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
Zusammenfassung: | The invention belongs to the technical field of sewage treatment, and particularly relates to a biquaternary ammonium bisulfonate degreasing agent as well as a synthesis method and application thereof. The synthesis method comprises the following steps: adding piperazine, sodium p-hydroxybenzenesulfonate, a formaldehyde solution and water into a four-neck flask, stirring, heating and carrying out reflux reaction to obtain a disulfonic acid bis-tertiary amine salt intermediate; carrying out reduced pressure distillation on the intermediate mixed solution until the intermediate mixed solution is dry to obtain a viscous solid, adding DMF (Dimethyl Formamide) and alkyl halide, carrying out heat preservation reaction, and evaporating to dryness by a rotary evaporator to obtain a disulfonic acid biquaternary ammonium salt crude product; adding ethyl acetate into the crude product, heating for dissolving, carrying out negative pressure suction filtration, cooling filtrate, separating out faint yellow solid, adding c |
---|