Rapid preparation method of metal-organic framework material (MOFs)

The invention relates to the field of inorganic functional materials, and discloses a rapid preparation method of a metal-organic framework material (MOFs). The preparation method comprises the following steps: dissolving the metal salt in the organic amine, dissolving the organic ligand in the amid...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Hauptverfasser: ZHU JUNPENG, KONG OURUI, LI JIJIA, JIANG GUANGSHEN, LI LICHAO, AN BAIGANG
Format: Patent
Sprache:chi ; eng
Schlagworte:
Online-Zugang:Volltext bestellen
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:The invention relates to the field of inorganic functional materials, and discloses a rapid preparation method of a metal-organic framework material (MOFs). The preparation method comprises the following steps: dissolving the metal salt in the organic amine, dissolving the organic ligand in the amide, adding the organic amine solution containing the metal salt into the amide solution containing the organic ligand, and obtaining the corresponding MOFs within 1 minute at normal temperature. The method has the advantage that the MOFs material is quickly obtained through a simple precipitation reaction at normal temperature. Compared with a water (solvent) thermal synthesis method, the method has the advantages of low energy consumption and rapid preparation, the used solvent can be recycled, and the method is very suitable for industrial production. 本发明涉及无机功能材料领域,公开一种金属-有机框架材料(MOFs)的快速制备方法。其制备方法是将金属盐溶于有机胺,有机配体溶于酰胺,将含有金属盐的有机胺溶液加入含有有机配体的酰胺溶液在常温下1分钟内即可得到相应的MOFs。本发明的优点:在常温下通过简单的沉淀反应快速获得MOFs材料。相比于水(溶剂)热合成方法,该方法具有低能耗、