Erbium-doped CsPbBr3 perovskite single crystal and preparation method thereof
The invention provides a preparation method of an erbium-doped CsPbBr3 perovskite single crystal, which comprises the following steps: preparing a precursor solution: dissolving CsBr, PbBr2 and ErBr3 in a DMSO solution, and stirring until the solution is transparent to prepare the precursor solution...
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Format: | Patent |
Sprache: | chi ; eng |
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Zusammenfassung: | The invention provides a preparation method of an erbium-doped CsPbBr3 perovskite single crystal, which comprises the following steps: preparing a precursor solution: dissolving CsBr, PbBr2 and ErBr3 in a DMSO solution, and stirring until the solution is transparent to prepare the precursor solution; pre-saturating the precursor solution: adding an anti-solvent into the precursor solution until CsPbBr3 precipitate appears, so as to obtain a pre-saturated solution; and single crystal growth: carrying out steam-assisted crystallization on the pre-saturated solution by using a mixed solvent of an anti-solvent and DMSO (Dimethylsulfoxide). The preparation method of the rare earth erbium-doped perovskite single crystal is used for preparing the Er < + >-doped CsPbBr3 perovskite single crystal, and a new method thought is provided for preparing the rare earth-doped perovskite single crystal.
本发明提供了一种铒掺杂CsPbBr3钙钛矿单晶的制备方法,包括:前驱液配置:以DMSO溶液溶解CsBr,PbBr2,ErBr3搅拌直至溶液透明,制成前驱体溶液;前驱液预饱和:将反溶剂加入所述前驱体溶液,直至出现CsPbBr3沉淀,得到预饱和溶液;单晶 |
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