Method for removing pungent smell in 1, 2-benzisothiazolin-3-one
The invention provides a method for removing pungent smell in 1, 2-benzisothiazolin-3-one, and relates to the technical field of fine chemical engineering, the method comprises the following steps: (1) alkali dissolution: adding BIT into water, and adjusting the pH to be alkaline by using alkali; (2...
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Format: | Patent |
Sprache: | chi ; eng |
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Zusammenfassung: | The invention provides a method for removing pungent smell in 1, 2-benzisothiazolin-3-one, and relates to the technical field of fine chemical engineering, the method comprises the following steps: (1) alkali dissolution: adding BIT into water, and adjusting the pH to be alkaline by using alkali; (2) reaction deodorization: adding a deodorant into the BIT alkali liquor, and reacting for 0.1-4 hours; (3) acidification: adding acid into the deodorized alkali liquor to adjust the pH value to 3-7, wherein the preferable pH value range is 4-7; and separating out BIT, filtering and drying to obtain an odorless BIT product.
本发明提供了一种去除1,2-苯并异噻唑啉-3-酮中刺激性气味的方法,涉及精细化工技术领域,本发明包括以下步骤:(1)碱溶:将BIT加入水中,用碱调pH至碱性;(2)反应除味:向BIT碱液中加入除味剂,反应0.1~4小时;(3)酸化:向除味后的碱液中加酸调pH至3~7,优选pH范围为4~7;BIT析出,过滤,干燥得无味的BIT产品。 |
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