Analysis method for separation and content determination of gamma-sultone and delta-sultone

The invention provides an analysis method for separation and content determination of gamma-sultone and delta-sultone, and belongs to the technical field of analysis and detection of fine chemical products. According to the method, different organic solvents are adopted to pre-treat AOS samples, then a gas chromatography-mass spectrometry technology is adopted to separate the AOS samples, and qualitative and quantitative analysis is carried out. The method disclosed by the invention is simple, rapid, reliable in nature determination and accurate in quantification, solvents used by the method are common solvents, the selection range is wide, the pretreatment process is simple and efficient, and used instruments are high in popularization degree and easy to popularize in a large area; not only is the quality of the product improved, but also the application prospect in the detection of the sultone substances in the AOS product is realized. 本发明提供了一种γ-磺内酯和δ-磺内酯的分离和含量测定的分析方法，属于精细化工产品分析检测的技术领域。本发明采用不同的有机溶剂对AOS样品进行前