Separation and preparation method of anti-cancer component in lepidium apetalum

The invention discloses a separation and preparation method of anti-cancer components in lepidium apetalum, and relates to the technical field of compound preparation and separation.The separation and preparation method of the anti-cancer components in the lepidium apetalum comprises the following s...

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Hauptverfasser: SUN SHIHAO, DU YURONG, MA JIANBIN, QI DESHENG, CUI YUNBIN
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention discloses a separation and preparation method of anti-cancer components in lepidium apetalum, and relates to the technical field of compound preparation and separation.The separation and preparation method of the anti-cancer components in the lepidium apetalum comprises the following steps that 1, raw materials are prepared; step 2, reflux extraction; step 3, vacuum concentration; step 4, gradient elution; and 5, screening and separating active components, namely separating vanillic acid, syringic acid, ethyl p-hydroxybenzoate and iso-aromatic oxalic acid from the active components. The preparation method has the beneficial effects that anti-cancer components such as vanillic acid, syringic acid, ethyl p-hydroxybenzoate and iso-aromatic oxalic acid in the lepidium apetalum can inhibit the growth of cancer cells, and the purity of the obtained compound is relatively high through separation preparation. 一种钝叶独行菜中抗癌成分的分离及制备方法,涉及化合物制备分离的技术领域,钝叶独行菜中抗癌成分的分离及制备方法包括以下步骤:步骤一、准备原料;步骤二、回流提取;步骤三、减压浓缩;步骤四、梯度洗