Method for preparing anisotropic flexible ionic liquid double-gel particles with adjustable morphology based on seed polymerization method

The invention relates to a method for preparing anisotropic flexible ionic liquid double-gel particles with adjustable morphology based on a seed polymerization method. According to the technical scheme, polymethyl methacrylate is used as a network, hydrophobic ionic liquid 1-butyl-3-methylimidazoli...

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Hauptverfasser: LIU DONG, WU QIONG, HE DONGQING, ZHAO SHUJIE, BEN CHUXUAN, SONG ZHINING
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention relates to a method for preparing anisotropic flexible ionic liquid double-gel particles with adjustable morphology based on a seed polymerization method. According to the technical scheme, polymethyl methacrylate is used as a network, hydrophobic ionic liquid 1-butyl-3-methylimidazolium hexafluorophosphate is used as a dispersion medium, prepared ionic liquid gel microspheres IL and PMMA are used as seeds, gamma-methacryloxypropyltrimethoxysilane MPS is used as a monomer, and the polymer microspheres are prepared through a hydrothermal method. Flexible ionic liquid double-gel particles are synthesized by adopting a seed emulsion polymerization induced phase separation method, and various spherical, hamburger-shaped, snowman-shaped and reverse-hamburger-shaped anisotropic gel particles are prepared through pH regulation and control. 本发明涉及一种基于种子聚合法制备形貌可调的各向异性柔性离子液体双凝胶微粒的方法。采用的技术方案是:以聚甲基丙烯酸甲酯为网络,疏水性离子液体1-丁基-3-甲基咪唑六氟磷酸盐为分散介质,制备的离子液体凝胶微球IL@PMMA为种子,γ-甲基丙烯酰氧基丙基三甲氧基硅烷MPS为单体,采用种子乳液聚合诱导相分离的方法合成柔性离子液体双凝胶微