Detection method of stiripentanol isomer
The invention relates to the technical field of analysis and detection, in particular to a detection method of a stiripentanol isomer. According to the method, high performance liquid chromatography is adopted for detection; chromatographic conditions of the high performance liquid chromatography ar...
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Format: | Patent |
Sprache: | chi ; eng |
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Zusammenfassung: | The invention relates to the technical field of analysis and detection, in particular to a detection method of a stiripentanol isomer. According to the method, high performance liquid chromatography is adopted for detection; chromatographic conditions of the high performance liquid chromatography are as follows: a chromatographic column is an octadecyl silane bonded silica gel chromatographic column; a mobile phase is methanol-0. 18 wt%-0.24 wt% of a sodium pentanesulfonate aqueous solution, and an isocratic elution mode is adopted for elution; the detector is an ultraviolet detector; the detection wavelength is 260 to 270 nm; the flow velocity is 1.0 to 1.3 ml/min. The detection method is high in sensitivity and good in specificity, can detect the stiripentanol and the cis-isomer of the stiripentanol, can be used for quality control of stiripentanol raw materials and preparations of the stiripentanol raw materials, and improves the medication safety of the stiripentanol.
本发明涉分析检测技术领域,尤其涉及一种司替戊醇异构体的检测方法。该方法,采 |
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