Preparation method of disperse blue 60 and derivative thereof
The invention provides a preparation method of disperse blue 60 and derivatives thereof, which comprises the following steps: a condensation reaction step: in the presence of an organic amine compound and/or monohydric alcohol, carrying out condensation reaction on 1, 4-diamino-2, 3-dicarboximide an...
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Format: | Patent |
Sprache: | chi ; eng |
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Zusammenfassung: | The invention provides a preparation method of disperse blue 60 and derivatives thereof, which comprises the following steps: a condensation reaction step: in the presence of an organic amine compound and/or monohydric alcohol, carrying out condensation reaction on 1, 4-diamino-2, 3-dicarboximide anthraquinone and gamma-alkoxy propylamine to obtain a condensation reaction product; a dilution step: diluting the condensation reaction product with dilution water to obtain a diluted product; and a crystallization step: crystallizing the condensation reaction product to obtain the disperse blue 60 and the derivative thereof. In the preparation process, chlorobenzene is not used for diluting water, so that the product reaches the standard in environmental protection index. In the preparation process, the use amount of ethanol in the condensation reaction can be reduced, the colored light distribution range of the disperse blue 60 is still wide, and the strength standard is still excellent. In the preparation proces |
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