Method for preparing parafuchsin
The invention belongs to the technical field of dyes, and particularly relates to a method for preparing parafuchsin, which comprises the following steps: by taking 4, 4 ', 4'-triaminotriphenylmethane as a substrate and manganese dioxide as a catalyst, carrying out oxidation reaction under...
Gespeichert in:
Hauptverfasser: | , , , |
---|---|
Format: | Patent |
Sprache: | chi ; eng |
Schlagworte: | |
Online-Zugang: | Volltext bestellen |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
Zusammenfassung: | The invention belongs to the technical field of dyes, and particularly relates to a method for preparing parafuchsin, which comprises the following steps: by taking 4, 4 ', 4'-triaminotriphenylmethane as a substrate and manganese dioxide as a catalyst, carrying out oxidation reaction under an acidic medium to obtain an intermediate product A, and carrying out alkalization treatment to obtain 4, 4 ', 4'-triaminotriphenylcarbinol. According to the method, the process difficulty of parafuchsin is solved, the 4, 4 ', 4'-triaminotriphenylmethane is converted into the 4, 4 ', 4'-triaminotriphenylcarbinol in a manner of combining the acidic medium and the catalyst, and the product purification is realized by utilizing the solubility difference.
本发明属于染料技术领域,具体涉及一种制备副品红的方法,以4,4',4"三氨基三苯甲烷为底物,以二氧化锰为催化剂,在酸性介质下氧化反应得到中间产物A,经碱化处理,得到4,4',4"三氨基三苯甲醇。本发明解决了副品红的工艺难点,利用酸性介质与催化剂相结合的方式将4,4',4"三氨基三苯甲烷转化为4,4',4"三氨基三苯甲醇,并利用溶解度差异实现产物提纯。 |
---|