GC-MSMS fingerprint spectrum method for pills

The invention relates to the technical field of traditional Chinese medicine detection, and discloses a GC-MSMS (Gas Chromatography-Mass Spectrometry-Mass Spectrometry) fingerprint spectrum method for pills. Comprising the following steps: preparing instruments and reagents, preparing a solution, op...

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Bibliographische Detailangaben
Hauptverfasser:	ZHOU YUCHUN, LAI GANG, XIAO YUN, ZHANG LEI, SUI RONGCHUN, MAI XI, CAI ZIXIAN, ZHANG DIPENG, FENG LIHUA, HU TINGGUO
Format:	Patent
Sprache:	chi ; eng
Schlagworte:	INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES MEASURING PHYSICS TESTING
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Beschreibung
Zusammenfassung:	The invention relates to the technical field of traditional Chinese medicine detection, and discloses a GC-MSMS (Gas Chromatography-Mass Spectrometry-Mass Spectrometry) fingerprint spectrum method for pills. Comprising the following steps: preparing instruments and reagents, preparing a solution, optimizing GC-MS (Gas Chromatography-Mass Spectrometer) analysis conditions, optimizing an experimental method and conditions, selecting a temperature rising program, determining a volatile component analysis result of the Guangdong life-prolonging pill, establishing a GC-MS fingerprint spectrum of the Guangdong life-prolonging pill, establishing the fingerprint spectrum of the Guangdong life-prolonging pill, and evaluating the similarity of the fingerprint spectrum of the Guangdong life-prolonging pill. According to the GC-MSMS fingerprint spectrum method for the pill, the fingerprint spectrum of the consolidating and life-prolonging pill is established, so that the quality of the consolidating and life-prolonging p