Preparation method of Pro-Pro-Val-Val

The invention belongs to the technical field of chemical analysis, and particularly relates to a preparation method of Pro-Pro-Val-Val. The preparation method of Pro-Pro-Val-Val comprises the following steps: a, extracting yellow water and an organic solvent, and concentrating an extracting solution...

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Hauptverfasser: LI YANGHUA, LIAO QINJIAN, GUO YAN, HU JIAO, LI SONGBAI, ZHAO DONG, LUO ZHU, SONG TINGFU, ZHENG JIA, WANG FANG, ZHOU HANLING
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creator LI YANGHUA
LIAO QINJIAN
GUO YAN
HU JIAO
LI SONGBAI
ZHAO DONG
LUO ZHU
SONG TINGFU
ZHENG JIA
WANG FANG
ZHOU HANLING
description The invention belongs to the technical field of chemical analysis, and particularly relates to a preparation method of Pro-Pro-Val-Val. The preparation method of Pro-Pro-Val-Val comprises the following steps: a, extracting yellow water and an organic solvent, and concentrating an extracting solution to obtain a crude extract; b, carrying out macroporous resin column chromatography on the crude extract, collecting an eluent containing Pro-Pro-Val-Val, and concentrating to obtain a crude product; and c, carrying out gel column chromatography on the crude product, collecting an eluent containing Pro-Pro-Val-Val, and concentrating to obtain the product. According to the method, Pro-Pro-Val-Val with the purity of 95% or above is separated from yellow water with complex components for the first time, a technical basis can be provided for separation and preparation of other peptide compounds in the yellow water, and meanwhile resource utilization of the yellow water is improved. 本发明属于化学分析技术领域,具体涉及Pro-Pro-Val-Val的制备方
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subjects CHEMISTRY
INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES
MEASURING
METALLURGY
ORGANIC CHEMISTRY
PEPTIDES
PHYSICS
TESTING
title Preparation method of Pro-Pro-Val-Val
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