Method for measuring content of allyl thionocarbamate

The invention belongs to the technical field of analysis and detection, and particularly relates to a method for determining the content of allyl thionocarbamate, which comprises the following steps: 1) establishing a working curve; 2) preparing a test solution; and 3) determination: sucking the test sample solution in the step S2, injecting the test sample solution into a high performance liquid chromatograph, and determining to obtain the content of the allyl thionocarbamate in the test sample. The synthesis method of the allyl thionocarbamate is simple and efficient, no organic by-products exist, only inorganic salt by-products are generated, the raw materials including the chloropropene, the ammonium thiocyanate and the isobutanol do not have conjugated double-bond absorption peaks, and the allyl thionocarbamate has the conjugated double-bond absorption peaks, so that the content of the allyl thionocarbamate can be measured through a high performance liquid chromatograph, and the content of the allyl thio