Aldehyde-group-containing naphthalimide derivative fluorescent probe as well as preparation method and application of aldehyde-group-containing naphthalimide derivative fluorescent probe
The invention relates to an aldehyde-group-containing naphthalimide derivative fluorescent probe as well as a preparation method and application thereof. The preparation method of the fluorescent probe comprises the following steps: reacting 4-bromo-1, 8-naphthalic anhydride (I) with n-butylamine to...
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| creator | LIU CHUANXIANG ZHANG ZIYI SHE QIUNAN ZHOU YAN MA LILI HU YAN |
| description | The invention relates to an aldehyde-group-containing naphthalimide derivative fluorescent probe as well as a preparation method and application thereof. The preparation method of the fluorescent probe comprises the following steps: reacting 4-bromo-1, 8-naphthalic anhydride (I) with n-butylamine to obtain a brominated naphthalimide derivative (II); reacting the brominated naphthalimide derivative (II) with acetohydroxamic acid to obtain a naphthalimide derivative (III) containing a hydroxyl group; the naphthalimide derivative (III) containing the hydroxyl group reacts with hexamethylenetetramine to obtain the naphthalimide derivative (IV) containing the aldehyde group and the hydroxyl group, and the fluorescent probe is used for preparing a fluorescent probe coating. Compared with the prior art, the invention provides a novel amino detection method aiming at the limitation that the existing detection method cannot quantitatively analyze the amine functionalization on the surface of the material. The effect o |
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The preparation method of the fluorescent probe comprises the following steps: reacting 4-bromo-1, 8-naphthalic anhydride (I) with n-butylamine to obtain a brominated naphthalimide derivative (II); reacting the brominated naphthalimide derivative (II) with acetohydroxamic acid to obtain a naphthalimide derivative (III) containing a hydroxyl group; the naphthalimide derivative (III) containing the hydroxyl group reacts with hexamethylenetetramine to obtain the naphthalimide derivative (IV) containing the aldehyde group and the hydroxyl group, and the fluorescent probe is used for preparing a fluorescent probe coating. Compared with the prior art, the invention provides a novel amino detection method aiming at the limitation that the existing detection method cannot quantitatively analyze the amine functionalization on the surface of the material. The effect o</description><language>chi ; eng</language><subject>ADHESIVES ; CHEMICAL PAINT OR INK REMOVERS ; CHEMISTRY ; COATING COMPOSITIONS, e.g. PAINTS, VARNISHES ORLACQUERS ; CORRECTING FLUIDS ; DYES ; FILLING PASTES ; HETEROCYCLIC COMPOUNDS ; INKS ; INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES ; MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FORELSEWHERE ; MEASURING ; METALLURGY ; MISCELLANEOUS APPLICATIONS OF MATERIALS ; MISCELLANEOUS COMPOSITIONS ; NATURAL RESINS ; ORGANIC CHEMISTRY ; PAINTS ; PASTES OR SOLIDS FOR COLOURING OR PRINTING ; PHYSICS ; POLISHES ; TESTING ; USE OF MATERIALS THEREFOR ; WOODSTAINS</subject><creationdate>2023</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20230526&DB=EPODOC&CC=CN&NR=116162061A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76547</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20230526&DB=EPODOC&CC=CN&NR=116162061A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>LIU CHUANXIANG</creatorcontrib><creatorcontrib>ZHANG ZIYI</creatorcontrib><creatorcontrib>SHE QIUNAN</creatorcontrib><creatorcontrib>ZHOU YAN</creatorcontrib><creatorcontrib>MA LILI</creatorcontrib><creatorcontrib>HU YAN</creatorcontrib><title>Aldehyde-group-containing naphthalimide derivative fluorescent probe as well as preparation method and application of aldehyde-group-containing naphthalimide derivative fluorescent probe</title><description>The invention relates to an aldehyde-group-containing naphthalimide derivative fluorescent probe as well as a preparation method and application thereof. The preparation method of the fluorescent probe comprises the following steps: reacting 4-bromo-1, 8-naphthalic anhydride (I) with n-butylamine to obtain a brominated naphthalimide derivative (II); reacting the brominated naphthalimide derivative (II) with acetohydroxamic acid to obtain a naphthalimide derivative (III) containing a hydroxyl group; the naphthalimide derivative (III) containing the hydroxyl group reacts with hexamethylenetetramine to obtain the naphthalimide derivative (IV) containing the aldehyde group and the hydroxyl group, and the fluorescent probe is used for preparing a fluorescent probe coating. Compared with the prior art, the invention provides a novel amino detection method aiming at the limitation that the existing detection method cannot quantitatively analyze the amine functionalization on the surface of the material. 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The preparation method of the fluorescent probe comprises the following steps: reacting 4-bromo-1, 8-naphthalic anhydride (I) with n-butylamine to obtain a brominated naphthalimide derivative (II); reacting the brominated naphthalimide derivative (II) with acetohydroxamic acid to obtain a naphthalimide derivative (III) containing a hydroxyl group; the naphthalimide derivative (III) containing the hydroxyl group reacts with hexamethylenetetramine to obtain the naphthalimide derivative (IV) containing the aldehyde group and the hydroxyl group, and the fluorescent probe is used for preparing a fluorescent probe coating. Compared with the prior art, the invention provides a novel amino detection method aiming at the limitation that the existing detection method cannot quantitatively analyze the amine functionalization on the surface of the material. The effect o</abstract><oa>free_for_read</oa></addata></record> |
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| subjects | ADHESIVES CHEMICAL PAINT OR INK REMOVERS CHEMISTRY COATING COMPOSITIONS, e.g. PAINTS, VARNISHES ORLACQUERS CORRECTING FLUIDS DYES FILLING PASTES HETEROCYCLIC COMPOUNDS INKS INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FORELSEWHERE MEASURING METALLURGY MISCELLANEOUS APPLICATIONS OF MATERIALS MISCELLANEOUS COMPOSITIONS NATURAL RESINS ORGANIC CHEMISTRY PAINTS PASTES OR SOLIDS FOR COLOURING OR PRINTING PHYSICS POLISHES TESTING USE OF MATERIALS THEREFOR WOODSTAINS |
| title | Aldehyde-group-containing naphthalimide derivative fluorescent probe as well as preparation method and application of aldehyde-group-containing naphthalimide derivative fluorescent probe |
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