Production equipment of oxamide derivative and use method of production equipment

According to the oxamide derivative production equipment and the use method thereof, the production equipment comprises a first reactor, a second reactor, a cooling chamber and a volatilization chamber, a trace vacuum pump and an air pipe are arranged in the volatilization chamber, the temperature o...

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1. Verfasser: SHANG MEIJIE
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:According to the oxamide derivative production equipment and the use method thereof, the production equipment comprises a first reactor, a second reactor, a cooling chamber and a volatilization chamber, a trace vacuum pump and an air pipe are arranged in the volatilization chamber, the temperature of air in the air pipe is controlled, temperature difference can be formed in the volatilization chamber, air flow in the volatilization chamber is accelerated, and formation of single crystals is promoted; in addition, the air exhaust speed is controlled by the micro vacuum pump, so that the output speed of a target product can be remarkably increased, the time required for preparing the oxamide derivative is shortened, the production efficiency is higher, the formation of a dark black complex single crystal is not influenced, the yield is not influenced, and the yield is high. 本发明一种草酰胺衍生物的生产设备及其使用方法,生产设备包括:第一反应器、第二反应器、冷却室、挥发室,挥发室内设置有微量真空泵及气管,控制气管中的气体温度,可在挥发室内形成温差,加速挥发室内空气流动,促进单晶的形成,加之通过微量真空泵控制抽气速度,可以显著提升目标产物的产出速度,