Process for preparation of 2-chloro-n-(1-cyanocyclopropyl)-5-[2 '-methyl-5'-(pentafluoroethyl)-4 '-(trifluoromethyl)-2'h-1, 3'-bipyrazol-4-yl] benzamide

The present invention relates to a process for the preparation of 2-chloro-N-(1-cyanocyclopropyl)-5-[2 '-methyl-5'-(pentafluoroethyl)-4 '-(trifluoromethyl)-2' H-1, 3 '-bipyrazol-4-yl] benzamide, i.e., a compound of formula (I), and to a process for the purification of said c...

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Bibliographische Detailangaben
Hauptverfasser: SCHEITHAUER HILDEGARD, FRANZ-JOSEF MEIS, OLEJNIK, BRITTA, LINDNER, WERNER, KEIL BIRGIT
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The present invention relates to a process for the preparation of 2-chloro-N-(1-cyanocyclopropyl)-5-[2 '-methyl-5'-(pentafluoroethyl)-4 '-(trifluoromethyl)-2' H-1, 3 '-bipyrazol-4-yl] benzamide, i.e., a compound of formula (I), and to a process for the purification of said compound of formula I. The invention also relates to a novel crystal form of the compound shown in the formula I. 本发明涉及一种用于制备2-氯-N-(1-氰基环丙基)-5-[2'-甲基-5'-(五氟乙基)-4'-(三氟甲基)-2'H-1,3'-联吡唑-4-基]苯甲酰胺,即式(I)化合物的方法以及一种用于纯化所述式I化合物的方法。本发明还涉及所述式I化合物的新晶型。