Method for preparing hollow ferroferric oxide nanoparticles

The invention discloses a method for preparing hollow ferroferric oxide nanoparticles. The method comprises the following specific steps: adding deionized water and a cinnamon extract in a certain volume ratio into a three-neck flask at room temperature, and carrying out ultrasonic dispersion and un...

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Hauptverfasser: LIU HONGYU, ZHU JING, ZHANG MAN, XU BO, QIN DANDAN, LONG YONGFENG, WANG MINYANG, YANG XUPENG, YANG JING, LIAO JIAWEI, TIAN TAIFU, LIU JIALE, ZHENG XINGNONG, LIU ZHI, ZHAO WENKAI, WU WENTAO, CHENG GUIGANG, SUN MINGZHU
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention discloses a method for preparing hollow ferroferric oxide nanoparticles. The method comprises the following specific steps: adding deionized water and a cinnamon extract in a certain volume ratio into a three-neck flask at room temperature, and carrying out ultrasonic dispersion and uniform mixing; after uniformly mixing, putting an iron source and the mixture into a hydrothermal kettle together, and reacting for a period of time at a certain temperature until the reaction is complete; and pouring out a product, carrying out magnetic separation, alternately cleaning the product obtained by magnetic separation with deionized water and ethanol for three to four times, carrying out suction filtration, preparing a suction filtration product and deionized water into a suspension, carrying out spray drying, and collecting a dried product to obtain the ferroferric oxide nano-particles. 本发明公开了一种制备空心四氧化三铁纳米颗粒的方法。具体步骤为:在室温下往三口烧瓶内加入一定体积比的去离子水和桂皮提取物,超声分散混合均匀;混合均匀后,将铁源与混合物一同放入水热釜,在一定温度下反应一段时间,等待反应完全;倒出产物进行磁性