Online preparation method of carbon nanowire electrode
The invention discloses a carbon nanowire electrode on-line preparation method which comprises the following steps: step 1, mounting a carbon nanowire electrode on a fixing mechanism arranged on a Z-axis connecting seat of a three-coordinate mobile platform, step 2, sleeving the carbon nanowire elec...
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Format: | Patent |
Sprache: | chi ; eng |
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Zusammenfassung: | The invention discloses a carbon nanowire electrode on-line preparation method which comprises the following steps: step 1, mounting a carbon nanowire electrode on a fixing mechanism arranged on a Z-axis connecting seat of a three-coordinate mobile platform, step 2, sleeving the carbon nanowire electrode with a liquid film mechanism arranged in an electro-deposition tank, step 3, carrying out electro-deposition on the carbon nanowire electrode, and step 4, carrying out electro-deposition on the carbon nanowire electrode. A KMnO4/KClO3/H2SO4 solution with a certain proportion is added to the closed loop position of the liquid film mechanism, the carbon nanowire electrode is connected with the positive electrode of a power source, the liquid film mechanism is connected with the negative electrode of the power source, and electrochemical anodizing treatment is conducted on the carbon nanowire electrode. Electrochemical anodizing treatment is carried out on the surface of the carbon nanowire electrode, residual i |
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