Method for determining content of n-hexane extract in polyethylene resin
The invention relates to a method for determining the content of n-hexane extract in polyethylene resin. The method comprises the following steps: step 1, classifying samples; 2, calibrating the content of the normal hexane extract of the standard sample; step 3, measuring a low-resolution pulse nuc...
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creator | WANG LI LI HONGMING ZU FENGHUA WANG YISEN WANG YONGGANG LI RONGBO |
description | The invention relates to a method for determining the content of n-hexane extract in polyethylene resin. The method comprises the following steps: step 1, classifying samples; 2, calibrating the content of the normal hexane extract of the standard sample; step 3, measuring a low-resolution pulse nuclear magnetic signal of the standard sample; 4, establishing a low-resolution pulse nuclear magnetic signal correction curve of the content of the n-hexane extract; 5, measuring the low-resolution pulse nuclear magnetic signal of the to-be-measured sample; and 6, calculating the content of the n-hexane extract of the sample to be detected by using the calibration curve and the low-resolution pulse nuclear magnetic signal value of the sample to be detected. According to the determination method provided by the invention, the use of a large amount of organic solvent in the existing weighing method test is avoided, the test time is shortened, the test steps are reduced, and the method has the characteristics of enviro |
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The method comprises the following steps: step 1, classifying samples; 2, calibrating the content of the normal hexane extract of the standard sample; step 3, measuring a low-resolution pulse nuclear magnetic signal of the standard sample; 4, establishing a low-resolution pulse nuclear magnetic signal correction curve of the content of the n-hexane extract; 5, measuring the low-resolution pulse nuclear magnetic signal of the to-be-measured sample; and 6, calculating the content of the n-hexane extract of the sample to be detected by using the calibration curve and the low-resolution pulse nuclear magnetic signal value of the sample to be detected. 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The method comprises the following steps: step 1, classifying samples; 2, calibrating the content of the normal hexane extract of the standard sample; step 3, measuring a low-resolution pulse nuclear magnetic signal of the standard sample; 4, establishing a low-resolution pulse nuclear magnetic signal correction curve of the content of the n-hexane extract; 5, measuring the low-resolution pulse nuclear magnetic signal of the to-be-measured sample; and 6, calculating the content of the n-hexane extract of the sample to be detected by using the calibration curve and the low-resolution pulse nuclear magnetic signal value of the sample to be detected. 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The method comprises the following steps: step 1, classifying samples; 2, calibrating the content of the normal hexane extract of the standard sample; step 3, measuring a low-resolution pulse nuclear magnetic signal of the standard sample; 4, establishing a low-resolution pulse nuclear magnetic signal correction curve of the content of the n-hexane extract; 5, measuring the low-resolution pulse nuclear magnetic signal of the to-be-measured sample; and 6, calculating the content of the n-hexane extract of the sample to be detected by using the calibration curve and the low-resolution pulse nuclear magnetic signal value of the sample to be detected. According to the determination method provided by the invention, the use of a large amount of organic solvent in the existing weighing method test is avoided, the test time is shortened, the test steps are reduced, and the method has the characteristics of enviro</abstract><oa>free_for_read</oa></addata></record> |
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subjects | INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES MEASURING PHYSICS TESTING |
title | Method for determining content of n-hexane extract in polyethylene resin |
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