Preparation and detection method of azo compound

The invention relates to a preparation and detection method of an azo compound, and belongs to the field of medicinal chemistry. The preparation method comprises the following steps: carrying out catalytic hydrogenation reaction and reoxidation reaction on raw materials to prepare a target compound. According to the preparation, analysis and detection method provided by the invention, the target compound can be well obtained, and the content of the target compound can be detected and analyzed, so that the medicine quality is controlled, and the medication safety is improved. 本发明涉及一种偶氮化合物的制备及检测方法，属于药物化学领域。所述制备方法包括原料经催化氢化反应，再氧化反应，制备得到目标化合物。本发明所提供的制备及分析检测方法，能够很好的获得目标化合物并且检测分析其含量，从而控制药品质量，提高用药安全性。