Production method of trans-2. 4-nonadienal
The invention discloses a production method of trans-2, 4-nonadienal, which comprises the following steps: by taking n-valeraldehyde, ethanol and vinyl ethyl ether as main raw materials, acetic acid as a solvent and calcium chloride as a water absorbent, carrying out quantitative reaction in a close...
Gespeichert in:
Hauptverfasser: | , , , , |
---|---|
Format: | Patent |
Sprache: | chi ; eng |
Schlagworte: | |
Online-Zugang: | Volltext bestellen |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
Zusammenfassung: | The invention discloses a production method of trans-2, 4-nonadienal, which comprises the following steps: by taking n-valeraldehyde, ethanol and vinyl ethyl ether as main raw materials, acetic acid as a solvent and calcium chloride as a water absorbent, carrying out quantitative reaction in a closed reaction kettle; the preparation method comprises the following steps: synthesizing 1, 1-diethoxypentane, 1, 1, 3-triethoxyheptane, 1, 1, 3-tetraethoxynonane, and finally hydrolyzing to generate the trans-2, 4-nonadienal. The preparation method comprises the following steps: synthesizing 1, 1-diethoxypentane, 1, 1, 3-triethoxyheptane and 1, 1, 3-tetraethoxynonane. Through repeated tests, trial production and production, a good effect is obtained; the product yield and quality are high, and the highest yield can reach 30%. The method is easy to operate, safe, environmentally friendly and suitable for large-scale industrial production.
本发明公开了一种反式-2.4-壬二烯醛的生产方法,本发明采用正戊醛与乙醇及乙烯基乙醚为主原料,乙酸作溶剂、氯化钙作吸水剂,在密闭的反应釜中定量反应,经过1.1- |
---|