High-throughput detection method for carbamates and thiolates thereof

The invention provides a high-throughput detection method for carbamates and thiolates thereof, and belongs to the technical field of detection methods. The MWCNTs (at) SiO2 (at) PANI novel solid-phase extraction adsorbent is used for purifying samples of traditional Chinese medicinal materials, tea leaves, mushrooms and the like, interference of complex matrixes in the traditional Chinese medicinal materials, the tea leaves, the mushrooms and the like can be effectively reduced, the material can be repeatedly used for multiple times after repeated alcohol-water washing, determination is carried out by adopting high performance liquid chromatography-mass spectrometry (HPLC-MS/MS), and the determination result is accurate. The efficient, accurate, simple and convenient rapid detection method for various carbamates and thio-compound pesticide residues in traditional Chinese medicinal materials, tea leaves and mushrooms is established, and the detection limit, the recovery rate and the precision of the method ar