PVDF-based composite film with double-layer structure and preparation method of PVDF-based composite film
The invention relates to a PVDF-based composite film with a double-layer structure and a preparation method of the PVDF-based composite film. The method comprises the following steps that Na0.5Bi4.5Ti4O15, Na2CO3 and TiO2 are calcined in molten salt at 900-1000 DEG C, and then impurities are removed...
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Format: | Patent |
Sprache: | chi ; eng |
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Zusammenfassung: | The invention relates to a PVDF-based composite film with a double-layer structure and a preparation method of the PVDF-based composite film. The method comprises the following steps that Na0.5Bi4.5Ti4O15, Na2CO3 and TiO2 are calcined in molten salt at 900-1000 DEG C, and then impurities are removed to obtain Na0.5Bi0.5TiO3 crystals; na0.5Bi0.5TiO3 crystals and PVDF powder are uniformly dispersed in an organic solvent, the volume ratio of the Na0.5Bi0.5TiO3 crystals to the PVDF powder is 3%-9%, and a turbid liquid is obtained; the PVDF powder is uniformly dispersed in an organic solvent to obtain a PVDF solution; and the turbid liquid and the PVDF solution are sequentially subjected to film forming through a tape casting method, a compound is obtained, the compound is subjected to heat preservation for 7-9 min at the temperature of 195-205 DEG C and then quenched in water at the temperature of 0-5 DEG C, and the PVDF-based composite film of the double-layer structure is obtained.
本发明一种双层结构的PVDF基复合薄膜及其制备方法,该方法 |
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