Preparation method of composite visible light catalyst graphene quantum dot/graphite-phase nitrogen carbide

The invention discloses a preparation method of a composite visible light catalyst graphene quantum dot/graphite phase nitrogen carbide, and solves the problem that the efficiency of degrading NO by g-C3N4 under visible light is relatively low. The method comprises the following steps: by taking cit...

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Hauptverfasser: WANG TENG, YU HESHENG, HUANG XIAOXIANG, NIE QIANQIAN, JIA LIUHU, CUI YUNPEI
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention discloses a preparation method of a composite visible light catalyst graphene quantum dot/graphite phase nitrogen carbide, and solves the problem that the efficiency of degrading NO by g-C3N4 under visible light is relatively low. The method comprises the following steps: by taking citric acid monohydrate CA as a raw material, pyrolyzing to prepare GQDs; then taking melamine as a raw material, and calcining to prepare CN (Carbon Nitride); and then preparing the g-C3N4 composite photocatalyst GQDs/CN containing the graphene quantum dots GQDs by using a one-step hydrothermal method. Compared with a pure g-C3N4 photocatalyst, the GQDs/CN has the advantages that the NO degradation capability is improved, and the selectivity for generating NO3 is enhanced. A new thought is provided for application of the graphene quantum dot doped semiconductor catalyst in the field of environmental purification. 本发明公开了一种复合型可见光催化剂石墨烯量子点/石墨相碳化氮的制备方法,解决了g-C3N4可见光下降解NO效率较低的问题。本发明以一水合柠檬酸CA为原料,热解制备了GQDs;再以三聚氰胺melamine