Method for detecting disodium tetraborate in oxide removing agent

The invention provides a method for detecting disodium tetraborate in an oxide removing agent. The method comprises the following steps: (1) pretreating an oxide removing agent sample; (2) preparing a sample test solution; (3) selecting an element detection spectral line; (4) drawing a standard curv...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Hauptverfasser: ZHOU GUANNAN, HAN CHUNMEI, XIE WANLING, ZHANG XUEMEI, MA BAONING, TU YANYAN
Format: Patent
Sprache:chi ; eng
Schlagworte:
Online-Zugang:Volltext bestellen
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:The invention provides a method for detecting disodium tetraborate in an oxide removing agent. The method comprises the following steps: (1) pretreating an oxide removing agent sample; (2) preparing a sample test solution; (3) selecting an element detection spectral line; (4) drawing a standard curve; and (5) detecting the sample. According to the method disclosed by the invention, the problem of inapplicability of a national standard method to detection of disodium tetraborate in the oxide removal agent is solved by utilizing the inductively coupled plasma emission spectrum, and the method has the advantages of higher accuracy and precision, high standard recovery rate and good linear relationship, and can meet rapid and accurate production detection requirements. 本发明提供了一种检测除氧化物剂中四硼酸二钠的方法,包括以下步骤:①对除氧化物剂样品进行前处理;②制备样品试液;③选择元素检测谱线;④绘制标准曲线;⑤检测样品。本发明方法通过利用电感耦合等离子体发射光谱解决了国标方法对于检测除氧化物剂中四硼酸二钠的不适用性,且具有较高的准确度和精密度,加标回收率高,线性关系好,能够满足快速准确的生产检测要求。