Production of aromatic dicarboxylic acids

The present invention provides a process for generating water vapor in a process for preparing an aromatic dicarboxylic acid, the process for preparing an aromatic dicarboxylic acid comprising catalytic oxidation of a hydrocarbon precursor in an organic solvent, the process for generating water vapo...

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Bibliographische Detailangaben
Hauptverfasser: LEWIS ROBERT MATHERS, AKHILESH CHANDRA, ANUJ GUPTA, ANTONY PETER JOHN LIMBACH
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The present invention provides a process for generating water vapor in a process for preparing an aromatic dicarboxylic acid, the process for preparing an aromatic dicarboxylic acid comprising catalytic oxidation of a hydrocarbon precursor in an organic solvent, the process for generating water vapor comprising the steps of: i) heating a crude aromatic dicarboxylic acid slurry to form a crude aromatic dicarboxylic acid solution; ii) passing the crude aromatic dicarboxylic acid solution to a hydrogenation reactor; iii) passing the purified aromatic dicarboxylic acid solution from the hydrogenation reactor to a series of one or more crystallizers; and iv) passing heat from a crystallizer discharge stream from the series of one or more crystallizers to the water stream in the water vapor generator to generate water vapor. The invention also provides a device for implementing the method. 本发明提供了一种用于在制备芳族二羧酸的方法中生成水蒸气的方法,所述制备芳族二羧酸的方法包括烃前体在有机溶剂中的催化氧化,所述生成水蒸气的方法包括以下步骤:i)加热粗芳族二羧酸浆液以形成粗芳族二羧酸溶液;ii)将所述粗芳族二羧酸溶液传送至氢化反应器;iii