Method for extracting impurity-containing catalyst by sucralose esterification reaction
The invention relates to a method for extracting an impurity-containing catalyst by sucralose esterification reaction, which is characterized by comprising the following steps of: (1) pumping floccule in a floccule storage tank into a washing kettle, adding pure water for washing, stirring, and stan...
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Format: | Patent |
Sprache: | chi ; eng |
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Zusammenfassung: | The invention relates to a method for extracting an impurity-containing catalyst by sucralose esterification reaction, which is characterized by comprising the following steps of: (1) pumping floccule in a floccule storage tank into a washing kettle, adding pure water for washing, stirring, and standing for layering to obtain a floccule layer; (2) putting the floccule layer into a floccule extraction kettle, adding cyclohexane for extraction, standing, separating out an upper layer, returning the upper layer to the system for reuse, distilling and heating a middle layer and a lower layer to 85-95 DEG C to separate two phases to obtain lower-layer black impurity-containing organic tin acetate, and treating the upper layer in a sewage station; (3) adding liquid caustic soda with the concentration of 4-6% into a neutralization reaction kettle, heating to 85-90 DEG C, then adding the impurity-containing organic tin acetate for alkaline hydrolysis, and filtering to obtain a solid dibutyltin oxide crude product; an |
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