System and method for preparing 2, 3, 3, 3-tetrafluoropropene

The invention relates to a method for preparing 2, 3, 3, 3-tetrafluoropropene. The method comprises the following steps: respectively pumping 1, 1, 2, 3-tetrachloroethylene and hydrogen fluoride fromthe inlets of a first heater and a second heater, heating, introducing into a tubular reactor filled...

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Hauptverfasser: CONG XINXIN, ZHAI ZHIBING, TONG SHAOFENG, ZHANG JINGJING, ZHAO HENGJUN
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention relates to a method for preparing 2, 3, 3, 3-tetrafluoropropene. The method comprises the following steps: respectively pumping 1, 1, 2, 3-tetrachloroethylene and hydrogen fluoride fromthe inlets of a first heater and a second heater, heating, introducing into a tubular reactor filled with a fluorination catalyst, contacting at 300-400 DEG C for 10-30 seconds, cooling the obtained product, and introducing into a separation tank to separate; and pumping into the second heater again, heating, introducing into the tubular reactor filled with the elimination catalyst, contacting at350-500 DEG C for 3-10 seconds, washing with water, washing with alkali, drying and rectifying to obtain the target product 2, 3, 3, 3-tetrafluoropropene. Therefore, the method for preparing 2, 3, 3,3-tetrafluoropropene has the characteristics of small on-line reaction amount, low reaction temperature, safety, controllability, continuous production and low production cost. 一种制备2,3,3,3-四氟丙烯的方法,所述制备方法是将1,1,2,3-四氯乙烯、氟化氢分别从第一加