Application of aromatic hydrocarbon solvent in purification of p-phenylene diisocyanate and purification method

Application of aromatic hydrocarbon solvent in purification of p-phenylene diisocyanate and purification method

The invention provides application of an aromatic hydrocarbon solvent in purification of p-phenylene diisocyanate. A p-phenylene diisocyanate synthesis crude product is purified. The invention also provides a purification method of p-phenylene diisocyanate. The characteristic that the solubility of...

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Hauptverfasser: JI CHUANWU, LUO ZHICAI, ZHU XINJIANG, ZENG LEI
Format: Patent
Sprache:chi ; eng
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ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
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creator JI CHUANWU
LUO ZHICAI
ZHU XINJIANG
ZENG LEI
description The invention provides application of an aromatic hydrocarbon solvent in purification of p-phenylene diisocyanate. A p-phenylene diisocyanate synthesis crude product is purified. The invention also provides a purification method of p-phenylene diisocyanate. The characteristic that the solubility of the aromatic hydrocarbon solvent to p-phenylene diisocyanate and impurities in a p-phenylene diisocyanate crude product is different is utilized, the method comprises the following steps of: dissolving p-phenylene diisocyanate in an aromatic hydrocarbon solvent, adsorbing impurities, especially colored impurities, through activated carbon, performing filtering to remove the impurities, conducting cooling to separate out p-phenylene diisocyanate, and then performing filtering and drying to obtainthe final required product p-phenylene diisocyanate which is white in color and neat in appearance, thereby enhancing the market recognition degree of p-phenylene diisocyanate. Besides, the purification method disclosed by t
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subjects ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
title Application of aromatic hydrocarbon solvent in purification of p-phenylene diisocyanate and purification method
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