Method for detecting functional monomers in solvent type acrylic resin

The invention relates to the field of chemical analysis, and particularly provides a method for detecting functional monomers in solvent type acrylic resin. The method is characterized by comprising the following steps: (1) adding a basic monomer and a functional monomer into a solvent, adding an in...

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Bibliographische Detailangaben
Hauptverfasser: QIN GUOFEI, HU YA, WU JIE, JIA MENGHONG
Format: Patent
Sprache:chi ; eng
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Beschreibung
Zusammenfassung:The invention relates to the field of chemical analysis, and particularly provides a method for detecting functional monomers in solvent type acrylic resin. The method is characterized by comprising the following steps: (1) adding a basic monomer and a functional monomer into a solvent, adding an initiator, making reaction, keeping the temperature, and carrying out cooling and discharging to obtain a standard sample; (2) drying a standard sample, sending the standard sample into a pyrolysis gas chromatograph/mass spectrometer, and carrying out data determination; (3) calculating a relative correction factor of the functional monomer according to the measured peak areas of the main monomer and the functional monomer; and (4) according to the peak area of the functional monomer to be detected, calculating the content of the functional monomer to be detected by the average relative correction factor. 本发明涉及化学分析领域,更具体地,本发明提供了溶剂型丙烯酸树脂中功能单体的检测方法。本发明提供了溶剂型丙烯酸树脂中功能单体的检测方法,其特征在于,包括以下步骤:(1)将基本单体、功能单体加入到溶剂中,然后加入引发剂,反应,保温