Method and device for sublimation drying of maltol

The invention relates to a method and a device for sublimation drying of maltol. The device is characterized by comprising a sublimation kettle, wherein a dryer is additionally arranged in the front of the sublimation kettle; the outlet of the bottom part of the dryer is connected with the inlet of...

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Hauptverfasser: LIANG FANGYA, QIN JILOU
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creator LIANG FANGYA
QIN JILOU
description The invention relates to a method and a device for sublimation drying of maltol. The device is characterized by comprising a sublimation kettle, wherein a dryer is additionally arranged in the front of the sublimation kettle; the outlet of the bottom part of the dryer is connected with the inlet of the sublimation kettle through a pipeline; the outlet of the upper part of the dryer is connected with a condenser through a pipeline; and the condenser is connected with a distillate outlet groove through a pipeline. The method comprises the following steps: a, pouring coarse-crystalline maltol from a previous centrifugation section into the dryer, and heating the dryer to 60 to 80 DEG C through a pre-decompression method; and b, evaporating trichloromethane and water from the coarse-crystalline maltol, allowing the trichloromethane and the water to enter the condenser from the outlet of the upper part of the dryer, carrying out condensation, allowing condensed trichloromethane and condensed water to enter the dis
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The device is characterized by comprising a sublimation kettle, wherein a dryer is additionally arranged in the front of the sublimation kettle; the outlet of the bottom part of the dryer is connected with the inlet of the sublimation kettle through a pipeline; the outlet of the upper part of the dryer is connected with a condenser through a pipeline; and the condenser is connected with a distillate outlet groove through a pipeline. The method comprises the following steps: a, pouring coarse-crystalline maltol from a previous centrifugation section into the dryer, and heating the dryer to 60 to 80 DEG C through a pre-decompression method; and b, evaporating trichloromethane and water from the coarse-crystalline maltol, allowing the trichloromethane and the water to enter the condenser from the outlet of the upper part of the dryer, carrying out condensation, allowing condensed trichloromethane and condensed water to enter the dis</description><language>chi ; eng</language><subject>BLASTING ; CHEMISTRY ; DRYING ; DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM ; HEATING ; HETEROCYCLIC COMPOUNDS ; LIGHTING ; MECHANICAL ENGINEERING ; METALLURGY ; ORGANIC CHEMISTRY ; WEAPONS</subject><creationdate>2019</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=20190329&amp;DB=EPODOC&amp;CC=CN&amp;NR=109535113A$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25542,76289</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=20190329&amp;DB=EPODOC&amp;CC=CN&amp;NR=109535113A$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>LIANG FANGYA</creatorcontrib><creatorcontrib>QIN JILOU</creatorcontrib><title>Method and device for sublimation drying of maltol</title><description>The invention relates to a method and a device for sublimation drying of maltol. The device is characterized by comprising a sublimation kettle, wherein a dryer is additionally arranged in the front of the sublimation kettle; the outlet of the bottom part of the dryer is connected with the inlet of the sublimation kettle through a pipeline; the outlet of the upper part of the dryer is connected with a condenser through a pipeline; and the condenser is connected with a distillate outlet groove through a pipeline. The method comprises the following steps: a, pouring coarse-crystalline maltol from a previous centrifugation section into the dryer, and heating the dryer to 60 to 80 DEG C through a pre-decompression method; and b, evaporating trichloromethane and water from the coarse-crystalline maltol, allowing the trichloromethane and the water to enter the condenser from the outlet of the upper part of the dryer, carrying out condensation, allowing condensed trichloromethane and condensed water to enter the dis</description><subject>BLASTING</subject><subject>CHEMISTRY</subject><subject>DRYING</subject><subject>DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM</subject><subject>HEATING</subject><subject>HETEROCYCLIC COMPOUNDS</subject><subject>LIGHTING</subject><subject>MECHANICAL ENGINEERING</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><subject>WEAPONS</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2019</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZDDyTS3JyE9RSMxLUUhJLctMTlVIyy9SKC5NysnMTSzJzM9TSCmqzMxLV8hPU8hNzCnJz-FhYE1LzClO5YXS3AyKbq4hzh66qQX58anFBYnJqXmpJfHOfoYGlqbGpoaGxo7GxKgBAKwbK84</recordid><startdate>20190329</startdate><enddate>20190329</enddate><creator>LIANG FANGYA</creator><creator>QIN JILOU</creator><scope>EVB</scope></search><sort><creationdate>20190329</creationdate><title>Method and device for sublimation drying of maltol</title><author>LIANG FANGYA ; QIN JILOU</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_CN109535113A3</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>chi ; eng</language><creationdate>2019</creationdate><topic>BLASTING</topic><topic>CHEMISTRY</topic><topic>DRYING</topic><topic>DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM</topic><topic>HEATING</topic><topic>HETEROCYCLIC COMPOUNDS</topic><topic>LIGHTING</topic><topic>MECHANICAL ENGINEERING</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><topic>WEAPONS</topic><toplevel>online_resources</toplevel><creatorcontrib>LIANG FANGYA</creatorcontrib><creatorcontrib>QIN JILOU</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>LIANG FANGYA</au><au>QIN JILOU</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Method and device for sublimation drying of maltol</title><date>2019-03-29</date><risdate>2019</risdate><abstract>The invention relates to a method and a device for sublimation drying of maltol. The device is characterized by comprising a sublimation kettle, wherein a dryer is additionally arranged in the front of the sublimation kettle; the outlet of the bottom part of the dryer is connected with the inlet of the sublimation kettle through a pipeline; the outlet of the upper part of the dryer is connected with a condenser through a pipeline; and the condenser is connected with a distillate outlet groove through a pipeline. The method comprises the following steps: a, pouring coarse-crystalline maltol from a previous centrifugation section into the dryer, and heating the dryer to 60 to 80 DEG C through a pre-decompression method; and b, evaporating trichloromethane and water from the coarse-crystalline maltol, allowing the trichloromethane and the water to enter the condenser from the outlet of the upper part of the dryer, carrying out condensation, allowing condensed trichloromethane and condensed water to enter the dis</abstract><oa>free_for_read</oa></addata></record>
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subjects BLASTING
CHEMISTRY
DRYING
DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
HEATING
HETEROCYCLIC COMPOUNDS
LIGHTING
MECHANICAL ENGINEERING
METALLURGY
ORGANIC CHEMISTRY
WEAPONS
title Method and device for sublimation drying of maltol
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