Preparation method for super long structure metal ion-doped hydroxyapatite fiber material

A preparation method for a super long structure metal ion-doped hydroxyapatite fiber material comprises the following steps: (1) mixing a salt of a doping ion, a soluble calcium salt, guar gum and disodium hydrogen phosphate with deionized water to obtain a first mixed solution; (2) injecting the fi...

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Hauptverfasser: JIANG ZANLI, YANG HUI, YE SHEWEN, WU YANGJUN, YANG JIAQI
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:A preparation method for a super long structure metal ion-doped hydroxyapatite fiber material comprises the following steps: (1) mixing a salt of a doping ion, a soluble calcium salt, guar gum and disodium hydrogen phosphate with deionized water to obtain a first mixed solution; (2) injecting the first mixed solution into a strong alkali solution to form fiber gel, continuing to soak the obtainedfiber gel in the strong alkali solution for a period of time, and then drying to obtain a fiber precursor; and (3) calcining the fiber precursor to obtain a product, washing the product with deionizedwater, and drying to obtain the super-long structure metal ion-doped hydroxyapatite fiber material. The method has the advantages of simple preparation process, easy control of conditions, and no need of use of any templating agent. 公开了种超长结构金属离子掺杂羟基磷灰石纤维材料的制备方法,包括以下步骤:(1)将掺杂离子的盐、可溶性钙盐、瓜儿豆胶和磷酸氢二钠与去离子水混合得到第混合溶液;(2)将第混合溶液注入强碱溶液中形成纤维凝胶,得到的纤维凝胶继续在强碱溶液中浸泡定时间,然后干燥得到纤维前驱体;(3)将纤维前驱体煅烧得到产物,用去离子水洗涤产物,干燥后即得到所述超长结构金属离子掺杂羟基磷灰石纤维材料。该方法,