Boron magnesium co-doped VO2 powder, preparation method and application thereof
The invention discloses a boron magnesium co-doped VO2 powder, a preparation method and an application thereof. The preparation method comprises the following steps: dissolving a magnesium source anda boron source into hydrogen peroxide, and then adding a vanadium source, thereby preparing a V5+ com...
Gespeichert in:
Hauptverfasser: | , |
---|---|
Format: | Patent |
Sprache: | chi ; eng |
Schlagworte: | |
Online-Zugang: | Volltext bestellen |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
Zusammenfassung: | The invention discloses a boron magnesium co-doped VO2 powder, a preparation method and an application thereof. The preparation method comprises the following steps: dissolving a magnesium source anda boron source into hydrogen peroxide, and then adding a vanadium source, thereby preparing a V5+ complex hydrogel containing B3+ and Mg2+; adding a reducing agent into the V5+ complex hydrogel for performing reduction reaction, thereby acquiring a blue V4+ precursor solution; performing hydrothermal reaction on the V4+ precursor solution till generating sediment, cleaning and drying sediment, thereby acquiring an initial VO2 powder; calcining the initial VO2 powder under a protective gas atmosphere, thereby acquiring the boron magnesium co-doped VO2 powder. The invention can solve the problemof the prior art that a VO2 material with both low phase-transition temperature and high visible light transmittance cannot be acquired.
本发明公开了种硼镁共掺杂VO粉体及其制备方法和应用,其中,所述方法包括步骤:将镁源及硼源溶于双氧水中,再加入钒源,配制成含B和Mg的V配合物水凝胶;向V配合物水凝胶中加入还原剂 |
---|