Method for synthesizing 4-methyl-N-phenyl-N-(2-phenyl allyl) benzsulfamide compound
The invention specifically relates to a method for synthesizing a 4-methyl-N-phenyl-N-(2-phenyl allyl) benzsulfamide compound and belongs to the technical field of organic compound process application. The 4-methyl-N-phenyl-N-(2-phenyl allyl) benzsulfamide compound is a very significant chemical syn...
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Format: | Patent |
Sprache: | chi ; eng |
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Zusammenfassung: | The invention specifically relates to a method for synthesizing a 4-methyl-N-phenyl-N-(2-phenyl allyl) benzsulfamide compound and belongs to the technical field of organic compound process application. The 4-methyl-N-phenyl-N-(2-phenyl allyl) benzsulfamide compound is a very significant chemical synthesis intermediate and has very high application values. Water is adopted as a hydrogen source, bis(pinacolato) diboron is adopted as a water activator, the method is gentle in reaction condition, easy in raw material preparation, simple in reaction operation and high in yield, a novel method for simply and efficiently preparing the 4-methyl-N-phenyl-N-(2-phenyl allyl) benzsulfamide compound is creatively provided for a first time, and due to adoption of a metal palladium catalyst, conversion of the reaction can be efficiently achieved.
本发明具体涉及种制备种4-甲基-N-苯基-N-(2-苯基烯丙基)苯磺酰胺类化合物的合成方法,属于有机化合物工艺应用技术领域。4-甲基-N-苯基-N-(2-苯基烯丙基)苯磺酰胺类化合物是类非常重要的化工合成中间体,具有非常高的应用价值。本发明利用水作为氢源,联硼酸频那醇酯作为水的活化剂,反应条件温和,原料易制,反应操作简单,产率较高,首次创新地提出了种简单高效 |
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