Down-drain sludge microwave pyrolysis system and method for product collection

The invention relates to a down-drain sludge microwave pyrolysis system and method for product collection. The system comprises a microwave oven, a conical flask, a flask, a scrubbing gas flask, a quartz beaker and a thermocouple arranged in the quartz beaker; wherein the quartz beaker is correspond...

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Hauptverfasser: DAI QIANJIN, HU FENG, LIU QIANG, YANG YIYANG, TENG DAOXIANG, SHAO GUOSHUO, DENG WEI, LI KAIDI, LIU XINHUA, DAI WENJIN, SHAO JIAN, LI KERONG, MEI MAOFEI, SHAO HUANYU, ZHANG LINA, GUO XINGDAO, JIANG WEI, DAI QING, DAI ZILI, HU BIN
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention relates to a down-drain sludge microwave pyrolysis system and method for product collection. The system comprises a microwave oven, a conical flask, a flask, a scrubbing gas flask, a quartz beaker and a thermocouple arranged in the quartz beaker; wherein the quartz beaker is correspondingly arranged inside the microwave oven cavity; a quartz tube is fixedly inserted into the quartz tube passage, a purge gas inlet pipe is connected to the quartz tube, and a quartz cap is arranged on the quartz tube, a lower end of the quartz tube, the conical flask, a condenser, the flask, a resintube and the scrubbing gas bottle are connected in series. The method comprises the following steps: preparing samples by mixing; vertically arranging the quartz beaker containing the sample in the quartz tube; supplying nitrogen with a flow rate of 3L/min and purging for 10 minutes; then supplying nitrogen gas with a flow rate of 0.2 L/min to ensure the inert atmosphere during the pyrolysis process; carrying out the pyr