Preparation method of molybdic acid phenyl ester modified high ortho-position thermoset phenolic base hollow nanometer gradient activated carbon fibrous membrane

The invention discloses a preparation method of a molybdic acid phenyl ester modified high ortho-position thermoset phenolic base hollow nanometer gradient activated carbon fibrous membrane. The method comprises the following steps that a phenol compound, molybdic acid, an alcohol compound and hydro...

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Hauptverfasser: JIAO MINGLI, YANG KAI, ZHANG CAIYUN, REN DONGXUE, WEI PENG, SONG MENG, CAO JIAN, REN JINGRONG
Format: Patent
Sprache:chi ; eng
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Zusammenfassung:The invention discloses a preparation method of a molybdic acid phenyl ester modified high ortho-position thermoset phenolic base hollow nanometer gradient activated carbon fibrous membrane. The method comprises the following steps that a phenol compound, molybdic acid, an alcohol compound and hydrochloric acid are subjected to a constant temperature reaction under the temperature of 75-90 DEG C,an aldehyde compound is added, a heating boiling reaction is performed under the effect of a catalyst, a concentrated sulfuric acid solution is added dropwise, decompression and water extraction are performed to obtain molybdic acid phenyl ester modified high ortho-position phenolic resin; the molybdic acid phenyl ester modified high ortho-position phenolic resin is dissolved into an alcohol and aldehydes compound to have a reaction under the effect of another catalyst, and molybdic acid phenyl ester modified high ortho-position thermoset phenolic resin is obtained; the molybdic acid phenyl ester modified high ortho-p