Continuous naphthalene sulfonation reaction process
The invention discloses a continuous naphthalene sulfonation reaction process which sequentially comprises the following steps: feeding sulfuric acid and refined naphthalene into a primary sulfonationreactor, enabling a molar ratio of the primary sulfuric acid feed to refined naphthalene feed to be...
Gespeichert in:
Hauptverfasser: | , , |
---|---|
Format: | Patent |
Sprache: | chi ; eng |
Schlagworte: | |
Online-Zugang: | Volltext bestellen |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
Zusammenfassung: | The invention discloses a continuous naphthalene sulfonation reaction process which sequentially comprises the following steps: feeding sulfuric acid and refined naphthalene into a primary sulfonationreactor, enabling a molar ratio of the primary sulfuric acid feed to refined naphthalene feed to be 1:(1-1.1), and reacting for 40-50 minutes; feeding secondary sulfuric acid feed into a secondary sulfonation reactor, enabling a molar ratio of the secondary sulfuric acid feed to the primary sulfuric acid feed to be 1:(1.9-2.1), and mixing and reacting for 40-50 minutes; feeding third-time sulfuric acid feed into a third-stage sulfonation reactor, enabling a molar ratio of the third-time sulfuric acid feed to the primary sulfuric acid feed to be 1:(5-6), and mixing and reacting for 40-50 minutes; enabling the materials to enter a fourth-stage sulfonation reactor and a fifth-stage sulfonation reactor to respectively react for 60-80 minutes. The whole sulfonation process adopts continuous totally closed production, |
---|